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1 article(s) from Plutschack, Matthew B

Flow synthesis of a versatile fructosamine mimic and quenching studies of a fructose transport probe

Matthew B. Plutschack,
D. Tyler McQuade,
Giulio Valenti and
Peter H. Seeberger

Beilstein J. Org. Chem. 2013, 9, 2022–2027, doi:10.3762/bjoc.9.238

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Scheme 1: Batch synthesis of NBDM. a) NaNO₂, Amberlite IR-120 H⁺ (100 mL), 0 °C, water, 4 h. b) NH₂OH·HCl, Na...

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Scheme 2: The initial polymer-supported nitrite set up. A solution of glucosamine hydrochloride was passed ov...

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Scheme 3: Continuous flow synthesis of the key intermediate 1-amino-2,5-anhydro-D-mannose (3).

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Figure 1: Normalized NBDM absorption and emission, 40 µM and 2 µM.

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Figure 2: NBDM fluorescence from 1–40 µM (PBS buffer). The data set was plotted in OriginPro 8.6 and fitted u...

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Figure 3: Comparison of quenching 2 µM NBDM, as measured by fluorescence intensity of Trypan Blue, Bromopheno...

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Figure 4: Comparison of quenching 2 µM NBDM, as measured by fluorescence intensity of methionine and histidin...

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Published 07 Oct 2013

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